Spectroscopic Properties of Inorganic and Organometallic Compounds

Author: N N Greenwood

Publisher: Royal Society of Chemistry

ISBN: 184755492X

Category: Science

Page: 550

View: 3143

Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr

Spectroscopic Methods in Organic Chemistry, 2nd Edition 2007

Author: Manfred Hesse,Herbert Meier,Bernd Zeeh

Publisher: Georg Thieme Verlag

ISBN: 3131791322

Category: Science

Page: 450

View: 9790

Spectroscopic Methods in Organic Chemistry covers all aspects of modern spectroscopic methodology. It provides the necessary equipme nt for the application of spectroscopic methods in organic chemistry, as required as part of chemistry courses in all universities.T he following methods are explained and examples given:- UV/Vis Spectroscopy- Infrared (IR) and Raman Spectroscopy- Nuclear Magnetic Resonance Spectroscopy (NMR)- Mass spectrometry (MS)The layout and many tables help to introduce the reader to spectroscopy. The ext ensive and thorough approach makes the text the first choice both as a companion for the professional chemists and as a refresher co urse in practical spectroscopy. // The content of this e-book was originally published in 2007.

Spectroscopic Methods in Organic Chemistry, 2nd Edition 2007

Author: M. Hesse,H. Meier,B. Zeeh

Publisher: Georg Thieme Verlag

ISBN: 3131793724

Category: Science

Page: 450

View: 3629

Spectroscopic Methods in Organic Chemistry covers all aspects of modern spectroscopic methodology. It provides the necessary equipme nt for the application of spectroscopic methods in organic chemistry, as required as part of chemistry courses in all universities.T he following methods are explained and examples given:- UV/Vis Spectroscopy- Infrared (IR) and Raman Spectroscopy- Nuclear Magnetic Resonance Spectroscopy (NMR)- Mass spectrometry (MS)The layout and many tables help to introduce the reader to spectroscopy. The ext ensive and thorough approach makes the text the first choice both as a companion for the professional chemists and as a refresher co urse in practical spectroscopy. // The content of this e-book was originally published in 2007.

Nuclear Magnetic Resonance Spectroscopy of Boron Compounds

Author: Heinrich Nöth,Bernd Wrackmeyer

Publisher: Springer Science & Business Media

ISBN: 3642667570

Category: Science

Page: 464

View: 8638

The revolutionary impetus of the NMR methods in organic chemistry has parallels in the field of boron chemistry. lIB NMR spectroscopy provided a basis for the elucida tion of structures and reactions of the boron hydrides. However, although many studies have been carried out with the higher boranes, carboranes, metalloboranes, etc. , and although certain patterns have emerged, the correlation between the observed chemical shift and the assigned structural unit is still not fully understood. Therefore, predictions in this area are still rather limited, and semiquantitative interpretations are not yet pos sible. Several years ago Eaton and Lipscomb sUpImarized the status in this field in their book "NMR Studies of Boron Hydrides and Related Compounds" and a plethora of new data has accumulated since then. The book also contained material on simple bo rane derivatives, but they were not discussed in any detail. On the other hand many systematic studies, both synthetic and spectroscopic, have been conducted on these simple boron materials in the last decade. Thus a large amount of NMR information is available, not only on lIB but also on 1 H, 1 3 C, and 14 N. However, this information is widely scattered in the literature, and often the data are not discussed at all. It see med appropriate, therefore, to collect these data and to present them in one volume.

Nuclear Magnetic Resonance Spectroscopy

Author: John Henry Nelson

Publisher: Pearson College Division

ISBN: 9780130334510

Category: Science

Page: 464

View: 9736

This is the only how-to volume that investigates the spectroscopy of a variety of nuclides other than H and C in depth. It contains extensive reference material and numerous problems, most of which include real spectra. It is written to provide users with the knowledge necessary to choose the most appropriate experiment to obtain the best quality spectra with the ability to fully interpret the data. The book covers basic theory of NMR spectroscopy, spectrum measurement, the chemical shift and examples for selected nuclei, symmetry and NMR spectroscopy, spin-spin coupling and NMR spin systems, typical magnitude of selected coupling constants, nuclear spin relaxation, the nuclear overhauser effect, editing C NMR spectra, two-dimensional NMR spectroscopy, dynamic NMR spectroscopy, lanthanide shift reagents (LSR), NMR of solids. For NMR spectroscopists and analytical chemists.

Nuclear Magnetic Resonance Spectroscopy in Environmental Chemistry

Author: Mark A. Nanny,Roger A. Minear,Jerry A. Leenheer

Publisher: Oxford University Press

ISBN: 9780198025801

Category: Science

Page: 344

View: 9759

This book demonstrates the usefulness of NMR spectroscopy for a wide variety of applications in environmental science and technology. It contains a wealth of information relating to instrumentation, sample preparation, and data interpretation. The book is divided into three sections discussing contaminant interaction, solution and condensed-phase characterization, and nutrients and natural organic matter characterization. In addition to these in-depth chapters, an introductory overview provides the basic principles of solution and solid-state NMR spectroscopy. Each section also contains a discussion of advances in each area directly attributable to NMR spectroscopy. A final chapter suggests future directions for the deployment of this powerful technology in environmental science.

Nuclear Magnetic Resonance

Author: G. A. Webb

Publisher: Royal Society of Chemistry

ISBN: 0854043071

Category: Medical

Page: 564

View: 2084

For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage.

Progress in Nuclear Magnetic Resonance Spectroscopy

Author: J. W. Emsley,J Feeney,L H Sutcliffe

Publisher: Elsevier

ISBN: 1483281353

Category: Science

Page: 68

View: 8514

Progress in Nuclear Magnetic Resonance Spectroscopy, Part 1 is a two-chapter text that reviews significant developments in nuclear magnetic resonance (NMR) applications. The first chapter discusses NMR studies of molecules physisorbed on homogeneous surfaces. This chapter also describes the phase changes in the adsorbed layer detected by following the variation in the NMR parameters. The second chapter examines the process to obtain a plotted, data reduced Fourier transform NMR spectrum. This chapter highlights the pitfalls that can cause a decrease in information content in a NMR spectrum. The various steps involved in taking a free induction decay from a NMR spectrometer are also summarized. This book is of value to NMR spectroscopists, analytical chemists, and instrumentation students.

An Introduction to Spectroscopic Methods for the Identification of Organic Compounds

Nuclear Magnetic Resonance and Infrared Spectroscopy

Author: F. Scheinmann

Publisher: Elsevier

ISBN: 1483280772

Category: Science

Page: 212

View: 3726

An Introduction to Spectroscopic Methods for the Identification of Organic Compounds, Volume 1: Nuclear Magnetic Resonance and Infrared Spectroscopy discusses how spectral data can be translated into the structural formula of organic compounds and provides reference data and revised correlation tables for the initiated. The text describes high resolution nuclear magnetic resonance spectroscopy; the applications of nuclear magnetic resonance spectroscopy in organic chemistry; and correlation tables for nuclear magnetic resonance spectra. Nuclear magnetic resonance spectroscopy seminar problems and answers; the theoretical basis of infrared spectroscopy; and the applications of infrared spectroscopy to organic chemistry are also encompassed. The book further tackles infrared spectroscopic problems and answers, as well as correlation tables for infrared spectra.

NMR of Paramagnetic Molecules

Principles and Applications

Author: G. N. La Mar,W. Dew. Horrocks,R. H. Holm

Publisher: Elsevier

ISBN: 1483272451

Category: Science

Page: 694

View: 4891

NMR of Paramagnetic Molecules: Principles and Applications is a compendium of papers that discusses the physical principles behind the technique of nuclear magnetic resonance, as well as, evaluates the scope and limitation of the applications of NMR in chemistry and biology. These papers emphasize the applications of the technique in chemistry and biochemistry where it widely used, particularlyon NMR experiments in the liquid state. Some papers describe the theoretical factors governing the resonance position and linewidth, and then also interpret magnetic resonance parameters in terms of electronic structure. Another paper investigates the gap between the mathematical complexities of earlier experiments and the operational aspects of chemical information from the spectra. Examples show studies in biochemical molecules and process in events where contact interactions are present either as a result of intrinsic molecular paramagnetism or are just induced through the addition of suitable paramagnetic probes. One paper presents the definitive and controversial results involving stereochemistry and deuterium NMR. This collection of papers will prove useful for nuclear physicists, researchers, and academicians in the field of nuclear physics.

Nuclear Magnetic Resonance Spectroscopy

Author: Frank A. Bovey,Peter A. Mirau,H. S. Gutowsky

Publisher: Elsevier

ISBN: 0080916996

Category: Science

Page: 653

View: 4456

Nuclear Magnetic Resonance Spectroscopy, Second Edition focuses on two-dimensional nuclear magnetic resonance (NMR) spectroscopy, high resolution NMR of solids, water suppression, multiple quantum spectroscopy, and NMR imaging. The selection first takes a look at the fundamental principles and experimental methods. Discussions focus on the NMR phenomenon, dipolar broadening and spin-spin relaxation, nuclear electric quadrupole relaxation, saturation, magnetic shielding and chemical shift, magnetic field, transitions between the nuclear energy levels, and resolution and sensitivity considerations. The manuscript then ponders on chemical shift, coupling of nuclear spins, and nuclear relaxation and chemical rate processes. Topics include spin lattice relaxation, spin-spin relaxation, spin decoupling and associated techniques, and description and analysis of spin systems. The text examines two-dimensional NMR spectroscopy, macromolecules, and NMR of solids, including magic angle spinning, cross polarization, proton dipolar broadening, biopolymers, and chain motion in macromolecules. The selection is a valuable source of data for readers interested in nuclear magnetic resonance spectroscopy.

Magnetic Resonance Imaging of Carcinoma of the Urinary Bladder

Author: Jelle O. Barentsz,Frans M. J. Debruyne,J.H.J. Ruijs

Publisher: Springer Science & Business Media

ISBN: 940090651X

Category: Medical

Page: 136

View: 544

Carcinoma of the urinary bladder is a common (in the USA it is the fifth most common form of cancer in males and tenth most common form of cancer in females) malignan cy and one in which noninvasive staging by imaging plays such an important role. This book presents a complete approach to MR imaging of carcinoma of the urinary bladder from a detailed discussion of the value of MRI in the diagnosis of the urinary bladder to the history of the procedure. The technical discussion of the general principles of MRI including the optimal pulse sequences to be used and factors that influence the quality of images are included in this book. The safety factors are also presented along with contraindications. The application of a double surface coil with the field strength of O.5T provides the fine quality of the illustrations. The atlas of comparative anatomy by MRI on normal volunteers and post-mo'rtem specimens as well as MR images on patients with bladder tumors and post-surgery specimens is unique. The results of the clinical imaging stu dies in patients with carcinoma of the bladder, comparing the relative value of clinical staging, MR, CT and lymphography, are helpful in showing the advantages of MRI.

New Advances in Analytical Chemistry

Author: Atta-ur Rahman

Publisher: CRC Press

ISBN: 9780415272247

Category: Science

Page: 360

View: 1059

New Advances in Analytical Chemistry, Volume 3 presents recent developments in various spectroscopic techniques such as NMR spectroscopy and mass spectroscopy in the form of comprehensive reviews written by leading authorities in the field. With new and updated information. the book is invaluable to both research students and postdoctoral workers who wish to keep abreast of frontiers in analytical techniques. Each chapter provides a broad overall account of recent developments, so that the readers can stay current not only with the authors own contributions but also with contributions of other eminent scientists working in this area.