Spectroscopic Methods in Organic Chemistry, 2nd Edition 2007

Author: Manfred Hesse,Herbert Meier,Bernd Zeeh

Publisher: Georg Thieme Verlag

ISBN: 3131791322

Category: Science

Page: 450

View: 6673

Spectroscopic Methods in Organic Chemistry covers all aspects of modern spectroscopic methodology. It provides the necessary equipme nt for the application of spectroscopic methods in organic chemistry, as required as part of chemistry courses in all universities.T he following methods are explained and examples given:- UV/Vis Spectroscopy- Infrared (IR) and Raman Spectroscopy- Nuclear Magnetic Resonance Spectroscopy (NMR)- Mass spectrometry (MS)The layout and many tables help to introduce the reader to spectroscopy. The ext ensive and thorough approach makes the text the first choice both as a companion for the professional chemists and as a refresher co urse in practical spectroscopy. // The content of this e-book was originally published in 2007.

Spectroscopic Properties of Inorganic and Organometallic Compounds

Author: N N Greenwood

Publisher: Royal Society of Chemistry

ISBN: 184755492X

Category: Science

Page: 550

View: 7959

Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr

Spectroscopic Methods in Organic Chemistry, 2nd Edition 2007

Author: M. Hesse,H. Meier,B. Zeeh

Publisher: Georg Thieme Verlag

ISBN: 3131793724

Category: Science

Page: 450

View: 9689

Spectroscopic Methods in Organic Chemistry covers all aspects of modern spectroscopic methodology. It provides the necessary equipme nt for the application of spectroscopic methods in organic chemistry, as required as part of chemistry courses in all universities.T he following methods are explained and examples given:- UV/Vis Spectroscopy- Infrared (IR) and Raman Spectroscopy- Nuclear Magnetic Resonance Spectroscopy (NMR)- Mass spectrometry (MS)The layout and many tables help to introduce the reader to spectroscopy. The ext ensive and thorough approach makes the text the first choice both as a companion for the professional chemists and as a refresher co urse in practical spectroscopy. // The content of this e-book was originally published in 2007.

Nuclear Magnetic Resonance

Author: R K Harris

Publisher: Royal Society of Chemistry

ISBN: 1847553605

Category: Science

Page: 370

View: 2784

As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.

Nuclear Magnetic Resonance Spectroscopy

Author: John Henry Nelson

Publisher: Pearson College Division

ISBN: 9780130334510

Category: Science

Page: 464

View: 3404

This is the only how-to volume that investigates the spectroscopy of a variety of nuclides other than H and C in depth. It contains extensive reference material and numerous problems, most of which include real spectra. It is written to provide users with the knowledge necessary to choose the most appropriate experiment to obtain the best quality spectra with the ability to fully interpret the data. The book covers basic theory of NMR spectroscopy, spectrum measurement, the chemical shift and examples for selected nuclei, symmetry and NMR spectroscopy, spin-spin coupling and NMR spin systems, typical magnitude of selected coupling constants, nuclear spin relaxation, the nuclear overhauser effect, editing C NMR spectra, two-dimensional NMR spectroscopy, dynamic NMR spectroscopy, lanthanide shift reagents (LSR), NMR of solids. For NMR spectroscopists and analytical chemists.

Basic 1H- and 13C-NMR Spectroscopy

Author: Metin Balci

Publisher: Elsevier

ISBN: 9780080525532

Category: Science

Page: 430

View: 5609

Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful and theoretically complex analytical tool. Basic 1H- and 13C-NMR Spectroscopy provides an introduction to the principles and applications of NMR spectroscopy. Whilst looking at the problems students encounter when using NMR spectroscopy, the author avoids the complicated mathematics that are applied within the field. Providing a rational description of the NMR phenomenon, this book is easy to read and is suitable for the undergraduate and graduate student in chemistry. Describes the fundamental principles of the pulse NMR experiment and 2D NMR spectra Easy to read and written with the undergraduate and graduate chemistry student in mind Provides a rational description of NMR spectroscopy without complicated mathematics

Nuclear Magnetic Resonance Spectroscopy

An Introduction to Principles, Applications, and Experimental Methods

Author: Joseph B. Lambert,Eugene Mazzola,Clark D. Ridge

Publisher: Wiley

ISBN: 1119295238

Category: Science

Page: 480

View: 729

Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

Multinuclear NMR

Author: J. Mason

Publisher: Springer Science & Business Media

ISBN: 1461317835

Category: Science

Page: 660

View: 8224

With the power and range of modern pulse spectrometers the compass of NMR spec troscopy is now very large for a single book-but we have undertaken this. Our book covers the Periodic Table as multinuclear spectrometers do, and introductory chapters are devoted to the essentials of the NMR experiment and its products. Primary products are chemical shifts (including anisotropies), spin-spin coupling constants, and relaxation times; the ultimate product is a knowledge of content and constitution, dynamic as well as static. Our province is chemical and biochemical rather than physical or technical; only passing reference is made to metallic solids or unstable species, or to practical NMR spectroscopy. Our aim is depth as well as breadth, to explain the fundamental processes, whether of nuclear magnetic shielding, spin-spin coupling, relaxation, or the multiple pulse sequences that have allowed the development of high-resolution studies of solids, multidimensional NMR spectroscopy, techniques for sensitivity enhancement, and so on. This book therefore combines the functions of advanced textbook and reference book. For reasonably comprehensive coverage in a single volume we have sum marized the information in tables and charts, and included all leading references.

NMR of Paramagnetic Molecules

Principles and Applications

Author: G. N. La Mar,W. Dew. Horrocks,R. H. Holm

Publisher: Elsevier

ISBN: 1483272451

Category: Science

Page: 694

View: 7582

NMR of Paramagnetic Molecules: Principles and Applications is a compendium of papers that discusses the physical principles behind the technique of nuclear magnetic resonance, as well as, evaluates the scope and limitation of the applications of NMR in chemistry and biology. These papers emphasize the applications of the technique in chemistry and biochemistry where it widely used, particularlyon NMR experiments in the liquid state. Some papers describe the theoretical factors governing the resonance position and linewidth, and then also interpret magnetic resonance parameters in terms of electronic structure. Another paper investigates the gap between the mathematical complexities of earlier experiments and the operational aspects of chemical information from the spectra. Examples show studies in biochemical molecules and process in events where contact interactions are present either as a result of intrinsic molecular paramagnetism or are just induced through the addition of suitable paramagnetic probes. One paper presents the definitive and controversial results involving stereochemistry and deuterium NMR. This collection of papers will prove useful for nuclear physicists, researchers, and academicians in the field of nuclear physics.

Nuclear Magnetic Resonance

Author: G. A. Webb

Publisher: Royal Society of Chemistry

ISBN: 0854043071

Category: Medical

Page: 564

View: 8094

For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage.

Understanding NMR Spectroscopy

Author: James Keeler

Publisher: John Wiley & Sons

ISBN: 1119964938

Category: Science

Page: 526

View: 9067

This text is aimed at people who have some familiarity with high-resolution NMR and who wish to deepen their understanding of how NMR experiments actually ‘work’. This revised and updated edition takes the same approach as the highly-acclaimed first edition. The text concentrates on the description of commonly-used experiments and explains in detail the theory behind how such experiments work. The quantum mechanical tools needed to analyse pulse sequences are introduced set by step, but the approach is relatively informal with the emphasis on obtaining a good understanding of how the experiments actually work. The use of two-colour printing and a new larger format improves the readability of the text. In addition, a number of new topics have been introduced: How product operators can be extended to describe experiments in AX2 and AX3 spin systems, thus making it possible to discuss the important APT, INEPT and DEPT experiments often used in carbon-13 NMR. Spin system analysis i.e. how shifts and couplings can be extracted from strongly-coupled (second-order) spectra. How the presence of chemically equivalent spins leads to spectral features which are somewhat unusual and possibly misleading, even at high magnetic fields. A discussion of chemical exchange effects has been introduced in order to help with the explanation of transverse relaxation. The double-quantum spectroscopy of a three-spin system is now considered in more detail. Reviews of the First Edition “For anyone wishing to know what really goes on in their NMR experiments, I would highly recommend this book” – Chemistry World “…I warmly recommend for budding NMR spectroscopists, or others who wish to deepen their understanding of elementary NMR theory or theoretical tools” – Magnetic Resonance in Chemistry

Methodologies for Metabolomics

Experimental Strategies and Techniques

Author: Norbert W. Lutz,Jonathan V. Sweedler,Ron A. Wevers

Publisher: Cambridge University Press

ISBN: 1139619055

Category: Medical

Page: N.A

View: 7506

Metabolomics, the global characterisation of the small molecule complement involved in metabolism, has evolved into a powerful suite of approaches for understanding the global physiological and pathological processes occurring in biological organisms. The diversity of metabolites, the wide range of metabolic pathways and their divergent biological contexts require a range of methodological strategies and techniques. Methodologies for Metabolomics provides a comprehensive description of the newest methodological approaches in metabolomic research. The most important technologies used to identify and quantify metabolites, including nuclear magnetic resonance and mass spectrometry, are highlighted. The integration of these techniques with classical biological methods is also addressed. Furthermore, the book presents statistical and chemometric methods for evaluation of the resultant data. The broad spectrum of topics includes a vast variety of organisms, samples and diseases, ranging from in vivo metabolomics in humans and animals to in vitro analysis of tissue samples, cultured cells and biofluids.

How does MRI work?

An Introduction to the Physics and Function of Magnetic Resonance Imaging

Author: Dominik Weishaupt,Victor D. Köchli,Borut Marincek

Publisher: Springer Science & Business Media

ISBN: 3662078058

Category: Medical

Page: 138

View: 8773

From the reviews: 'The authors describe in English in the plainest fashion, and within hardly more than 100 pages, the theoretical and technical bases of magnetic resonance imaging. ...the book should be warmly recommended to anyone after they have become accustomed to MRI. In such circumstances this is a very comprehensive handbook, particularly useful as a reminder of the concepts of MRI.... a valuable technical handbook...' Surgical and Radiological Anatomy Vol. 26, Issue 3, 2004.

NMR Spectroscopy

Basic Principles, Concepts, and Applications in Chemistry

Author: Harald Günther

Publisher: Wiley

ISBN: 9780471952015

Category: Science

Page: 602

View: 5455

As with its predecessor, this edition uses a practical non-mathematical approach. Features a number of recent developments in the field including two-dimensional methods, solid state NMR and an enlarged treatment of Fourier Transform methods. Contains numerous two-color diagrams.

The theory of nuclear magnetic resonance

Author: Igorʹ Vladimirovich Aleksandrov

Publisher: N.A

ISBN: N.A

Category: Medical

Page: 197

View: 9756

The monograph is an attempt to expound certain basic contemorary concepts on the theory of nuclear magnetic resonance (NMR) (RMP). The literature list contains a number of books and also survey articles devoted to NMR. However, in all these works basic attention is given to graphic physical interpretation of phenomenon and to experimental problems of this method and its applications. Theoretical questions of NMR in available books and survey articles receive comparatively little space. In the monograph the authors ignore entirely questions connected with experimental techniques in NMR, referring the reader to cited works. Chapters I and II are devoted to theory of nuclear paramagnetic relaxation; Chapter III - questions of form of line in solid bodies; Chapter IV - theoretical questions of magnetic spectroscopy (chemical shift and spin-spin interaction in molecules); in Chapter V are considered certain questions connected with Bloch phenomenological equations. (Author).