Multinuclear Solid-State Nuclear Magnetic Resonance of Inorganic Materials

Author: Kenneth J.D. MacKenzie,M.E. Smith

Publisher: Elsevier

ISBN: 9780080537108

Category: Science

Page: 748

View: 1250

Techniques of solid state nuclear magnetic resonance (NMR) spectroscopy are constantly being extended to a more diverse range of materials, pressing into service an ever-expanding range of nuclides including some previously considered too intractable to provide usable results. At the same time, new developments in both hardware and software are being introduced and refined. This book covers the most important of these new developments. With sections addressed to non-specialist researchers (providing accessible answers to the most common questions about the theory and practice of NMR asked by novices) as well as a more specialised and up-to-date treatment of the most important areas of inorganic materials research to which NMR has application, this book should be useful to NMR users whatever their level of expertise and whatever inorganic materials they wish to study.

Annual Reports on NMR Spectroscopy

Author: Graham A. Webb

Publisher: Academic Press

ISBN: 0128003294

Category: Science

Page: 248

View: 2371

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. This volume of Annual Reports on NMR Spectroscopy focuses on the analytical tool used by chemists and physicists and includes topics such as Profiling of Food Samples, Recent Advances in Solution NMR Studies and Magic Angle Spinning NMR Studies of Protein Assemblies

Emerging Applications of Nanoparticles and Architectural Nanostructures

Current Prospects and Future Trends

Author: Abdel Salam Hamdy Makhlouf,Ahmed Barhoum

Publisher: William Andrew

ISBN: 0128135166

Category: Science

Page: 668

View: 1659

Emerging Applications of Nanoparticles and Architecture Nanostructures: Current Prospects and Future Trends discusses the most important current applications of nanoparticles and architecture nanostructures in a comprehensive, detailed manner. The book covers major applications of nanoparticles and architecture nanostructures, taking into account their unusual shapes and high surface areas. In particular, coverage is given to applications in aerospace, automotive, batteries, sensors, smart textile design, energy conversion, color imaging, printing, computer chips, medical implants, pharmacy, cosmetics, and more. In addition, the book discusses the future of research in these areas. This is a valuable reference for both materials scientists, chemical and mechanical engineers working both in R&D and academia who want to learn more on how nanoparticles and nanomaterials are commercially applied. Provides an in-depth look at the properties of nanoparticles and architecture nanostructures in terms of their applicability for industrial uses Analyzes the most recent advances and industrial applications of different types of nanoparticles and architecture nanostructures, taking into account their unusual structures and compositions Identifies novel nanometric particles and architectures that are of particular value for applications and the techniques required to use them effectively

Nuclear Magnetic Resonance

Author: G A Webb

Publisher: Royal Society of Chemistry

ISBN: 1847553788

Category: Science

Page: 622

View: 5186

As a spectroscopic method, Nuclear Magnetic Resonance (NMR) has seen spectacular growth over the past two decades, both as a technique and in its applications. Today the applications of NMR span a wide range of scientific disciplines, from physics to biology to medicine. Each volume of Nuclear Magnetic Resonance comprises a combination of annual and biennial reports which together provide comprehensive of the literature on this topic. This Specialist Periodical Report reflects the growing volume of published work involving NMR techniques and applications, in particular NMR of natural macromolecules which is covered in two reports: "NMR of Proteins and Acids" and "NMR of Carbohydrates, Lipids and Membranes". For those wanting to become rapidly acquainted with specific areas of NMR, this title provides unrivalled scope of coverage. Seasoned practitioners of NMR will find this an in valuable source of current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading authorities in the relevant subject areas, the series creates a unique service for the active research chemist, with regular, in-depth accounts of progress in particular fields of chemistry. Subject coverage within different volumes of a given title is similar and publication is on an annual or biennial basis.

Structure Elucidation in Organic Chemistry

The Search for the Right Tools

Author: Maria-Magdalena Cid,Jorge Bravo

Publisher: John Wiley & Sons

ISBN: 3527664637

Category: Science

Page: 552

View: 8058

Intended for advanced readers, this is a review of all relevant techniques for structure analysis in one handy volume. As such, it provides the latest knowledge on spectroscopic and related techniques for chemical structure analysis, such as NMR, optical spectroscopy, mass spectrometry and X-ray crystallography, including the scope and limitation of each method. As a result, readers not only become acquainted with the techniques, but also the advantages of the synergy between them. This enables them to choose the correct analytical method for each problem, saving both time and resources. Special emphasis is placed on NMR and its application to absolute configuration determination and the analysis of molecular interactions. Adopting a practical point of view, the author team from academia and industry guarantees both solid methodology and applications essential for structure determination, equipping experts as well as newcomers with the tools to solve any structural problem.


Proceedings of the Unified International Technical Conference on Refractories, November 8-11, 2005, Orlando, Florida, USA, 9th Biennial Worldwide Congress on Refractories

Author: Jeffrey D. Smith

Publisher: Wiley-American Ceramic Society

ISBN: 9781574982657

Category: Technology & Engineering

Page: 1040

View: 1318

This collection of over 200 papers from the 9th Biennial Worldwide Congress on Refractories is broad-ranging and diverse in perspective. Topics include steelmaking refractories, castable technology, global refractories education and technology and industrial applications. Numerous papers are from representatives from major international steel companies.

Water in Nominally Anhydrous Minerals

Author: Hans Keppler,J. R. Smyth

Publisher: Mineralogical Society of Amer


Category: Science

Page: 478

View: 5794

"The review chapters in this volume were the basis for a four day short course on Water in ..., held in Verbania, Lago Maggiore, Italy (October 1-4, 2006)"--P. [v].

Solid-state NMR Spectroscopy of Inorganic Materials

Author: John J. Fitzgerald

Publisher: Amer Chemical Society

ISBN: 9780841236028

Category: Science

Page: 422

View: 1956

This book strikes a balance between state-of-the-art solid-state NMR techniques and the applications of these techniques to problems in materials science. The applications focus on modern inorganic materials such as metal oxides, catalysts, zeolites, glasses, ceramics, semiconductors, ion conductors, superconductors, and composites. The book features chapters on multiple-quantum MAS NMR, dynamic-angle spinning NMR for quadrupolar nuclides, and two-dimensional NMR methods. It includes an introductory chapter that provides an a thorough and integrated overview of the field, complete with numerous references.

Analytical Instrumentation Handbook

Author: Jack Cazes

Publisher: CRC Press

ISBN: 9780849390395

Category: Science

Page: 1064

View: 6650

Compiled by the editor of Dekker's distinguished Chromatographic Science series, this reader-friendly reference is as a unique and stand-alone guide for anyone requiring clear instruction on the most frequently utilized analytical instrumentation techniques. More than just a catalog of commercially available instruments, the chapters are wri

The Multinuclear Approach to NMR Spectroscopy

Author: J.B. Lambert,F.G. Riddell

Publisher: Springer Science & Business Media

ISBN: 9400971303

Category: Mathematics

Page: 548

View: 5684

The field of nuclear magnetic resonance has experienced a number of spectacular developments during the last decade. Fourier transform methodology revolutionized signal acquisition capabilities. Superconducting magnets enhanced sensitivity and produced considerable improvement in spectral dispersion. In areas of new applicat ions, the life sciences particularly bene fited from these developments and probably saw the largest increase in usage. NMR imaging promises to offer a noninvasive alternative to X rays. High resolution is now achievable with solids, through magic angle spinning and cross polarization, so that the powers of NMR are applicable to previously intractable materials such as polymers, coal, and other geochemicals. The ease of obtaining relaxation times brought an important fourth variable, after the chemical shift, the coupling constant, and the rate constant, to the examination of structural and kinetic problems i~ all fields. Software development, particularly in the area of pulse sequences, created a host of useful tech niques, including difference decoupling and difference nuclear Overhauser effect spectra, multidimensional displays, signal enhancement (INEPT), coupling constant analysis for connectivity (INADEQUATE), and observation of specific structural classes such as only quaternary carbons. Finally, hardware development gave us access to the entire Periodic Table, to the particular advan tage of the inorganic and organometallic chemist. At the NATO Advanced Study Institute at Stirling, Scotland, the participants endeavored to examine all these advances, except imaging, from a multidisciplinary point of view.

Multinuclear Magnetic Resonance in Liquids and Solids — Chemical Applications

Author: P. Granger,Robin K. Harris

Publisher: Springer Science & Business Media

ISBN: 9400921497

Category: Science

Page: 476

View: 4002

The idea of this NATO school was born during philosophical discussions with Dr Brevard on the present and future of NMR during a night walk under the palm trees in Biskra during a seminar held in this oasis. It was clear for us that the recent progress in the field of NMR, especially inverse spectroscopy and the development of MAS, was opening new perspectives for chemists. We realised also that organometallic and inorganic chemists were not clearly informed about the potentialities of all the new methods. NA TO, with its summer schools, was offering a good opportunity to propose to the chemical community a session where those problems would be largely developped. This School is then the prolongation of the two previous ones: Palermo in 1976 on "the less receptive nuclei" and Stirling in 1982 on "the multinuclear approach to NMR spectroscopy" . It was divided into two sub-sessions: NMR in the liquid state and NMR in the solid state. This is reflected in the book organization. As indicated by the title of this School, we were mainly concerned with the methodological aspects of multinuclear NMR. If many examples are given, they appear only as a support for the understanding of the theory or in explanation of some practical aspects of the different experiments. Each domain is introduced by a lecture which presents selected examples.

Spectroscopic Properties of Inorganic and Organometallic Compounds

Author: G Davidson,E A V Ebsworth

Publisher: Royal Society of Chemistry


Category: Science

Page: 480

View: 8718

Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers.

Comprehensive Organometallic Chemistry III

From Fundamentals to Applications

Author: D. M. P. Mingos,Gerard Parkin

Publisher: Pergamon

ISBN: 9780080445908

Category: Science

Page: 9000

View: 9980

Comprehensive Organometallic Chemistry, 3rd Edition (COMC-III), is aimed at the specialist and non-specialist alike. It covers the major developments in the field in a carefully presented way with extensive cross-references. COMC-III provides a clear and comprehensive overview of developments since 1993 and attempts to predict trends in the field over the next ten years. Applications of organometallic chemistry continue to expand and this has been reflected by the significant increase in the number of volumes devoted to applications in COMC-III. Organic chemists have edited the volumes on organometallic chemistry towards organic synthesis - this is now organized by reaction type so as to be readily accessible to the organic community. Like its predecessors, COMC (1982) and COMC-II (1995), this new work is the essential reference text for any chemist or technologist who needs to use or apply organometallic compounds. Also available online via ScienceDirect (2006) - featuring extensive browsing, searching, and internal cross-referencing between articles in the work, plus dynamic linking to journal articles and abstract databases, making navigation flexible and easy. For more information, pricing options and availability visit * Presents a comprehensive overview of the major developments in the field since 1993 providing general and significant insights. * Highlights the expansion of applications in organometallic chemistry with a strong organic synthesis focus. * Provides a structured first point of entry to the key literature and background material for those planning research, teaching and writing about the area.

Solid state NMR II

Inorganic matter

Author: Bernhard Blümich,P. Diehl,Ekkehard Fluck,H. Günther

Publisher: Springer Verlag


Category: Science

Page: 215

View: 6659

NMR Spectroscopy in Liquids and Solids

Author: Vladimir I. Bakhmutov

Publisher: CRC Press

ISBN: 148226272X

Category: Medical

Page: 360

View: 8636

NMR Spectroscopy in Liquids and Solids provides an introduction of the general concepts behind Nuclear Magnetic Resonance (NMR) and its applications, including how to perform adequate NMR experiments and interpret data collected in liquids and solids to characterize molecule systems in terms of their structure and dynamics. The book is composed of ten chapters. The first three chapters consider the theoretical basis of NMR spectroscopy, the theory of NMR relaxation, and the practice of relaxation measurements. The middle chapters discuss the general aspects of molecular dynamics and their relationships to NMR, NMR spectroscopy and relaxation studies in solutions, and special issues related to NMR in solutions. The remaining chapters introduce general principles and strategies involved in solid-state NMR studies, provide examples of applications of relaxation for the determination of molecular dynamics in diamagnetic solids, and discuss special issues related to solid state NMR— including NMR relaxation in paramagnetic solids. All chapters are accompanied by references and recommended literature for further reading. Many practical examples of multinuclear NMR and relaxation experiments and their interpretations are also presented. The book is ideal for scientists new to NMR, students, and investigators working in the areas of chemistry, biochemistry, biology, pharmaceutical sciences, or materials science.