Experimental Organic Chemistry: A Miniscale and Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Cengage Learning

ISBN: 1439049149

Category: Science

Page: 960

View: 1690

Providing even more emphasis on inquiry-based learning, a new green experiment, and more than a dozen new discovery experiments, this Fifth Edition of Gilbert and Martin's proven EXPERIMENTAL ORGANIC CHEMISTRY contains procedures for both miniscale (also known as small scale) and microscale users. The manual first covers equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence. Chapters show students how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. A bioorganic experiment in Chapter 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.

Experimental Organic Chemistry: A Miniscale & Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Cengage Learning

ISBN: 1305687876

Category: Science

Page: 960

View: 2086

Perform chemistry experiments with skill and confidence in your organic chemistry lab course with this easy-to-understand lab manual. EXPERIMENTAL ORGANIC CHEMISTRY: A MINISCALE AND MICROSCALE APPROACH, Sixth Edition first covers equipment, record keeping, and safety in the laboratory, then walks you step by step through the laboratory techniques you'll need to perform all experiments. Individual chapters show you how to use the techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. New experiments in Chapter 17 and 18 demonstrate the potential of chiral agents in fostering enantioselectivity and of performing solvent-free reactions. A bioorganic experiment in Chapter 24 gives you an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.

Experimental Organic Chemistry

A Miniscale & Microscale Approach

Author: John C. Gilbert,Stephen F. Martin

Publisher: Brooks/Cole Publishing Company

ISBN: N.A

Category: Science

Page: 927

View: 9778

This proven and well-tested laboratory manual for organic chemistry students contains procedures for both miniscale (also known as small scale) and microscale users. This lab manual gives students all the necessary background to enter the laboratory with the knowledge to perform the experiments with confidence. For the microscale labs, experiments were chosen to provide tangible quantities of material, which can then be analyzed. Chapters 1-2 introduce students to the equipment, record keeping, and safety of the laboratory. Chapters 3-6, and 8 are designed to introduce students to laboratory techniques needed to perform all experiments. In Chapters 7 and 9 through 20, students are required to use the techniques to synthesize compounds and analyze their properties. In Chapter 21, students are introduced to multi-step syntheses of organic compounds, a practice well known in chemical industry. In Chapter 23, students are asked to solve structures of unknown compounds. The new chapter 24 introduces a meaningful experiment into the textbook that reflects the increasing emphasis on bioorganic chemistry in the sophomore-level organic lecture course. This experiment not only gives students the opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide but also provides valuable experience regarding the role of protecting groups in effecting synthetic transformations with multiple functionalized molecules.

Experimental Organic Chemistry

Author: Philippa B. Cranwell,Laurence M. Harwood,Christopher J. Moody

Publisher: John Wiley & Sons

ISBN: 1118683412

Category: Science

Page: 688

View: 1505

The definitive guide to the principles and practice of experimental organic chemistry - fully updated and now featuring more than 100 experiments The latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. All sections have been updated to reflect new techniques, equipment and technologies, and the text has been revised with an even sharper focus on practical skills and procedures. The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis. The second half contains step-by-step experimental procedures, each one illustrating a basic principle, or important reaction type. Tried and tested over almost three decades, over 100 validated experiments are graded according to their complexity and all are chosen to highlight important chemical transformations and to teach key experimental skills. New sections cover updated health and safety guidelines, additional spectroscopic techniques, electronic notebooks and record keeping, and techniques, such as semi-automated chromatography and enabling technologies such as the use of microwave and flow chemistry. New experiments include transition metal-catalysed cross-coupling, organocatalysis, asymmetric synthesis, flow chemistry, and microwave-assisted synthesis. Key aspects of this third edition include: Detailed descriptions of the correct use of common apparatus used in the organic laboratory Outlines of practical skills that all chemistry students must learn Highlights of aspects of health and safety in the laboratory, both in the first section and throughout the experimental procedures Four new sections reflecting advances in techniques and technologies, from electronic databases and information retrieval to semi-automated chromatography More than 100 validated experiments of graded complexity from introductory to research level A user-friendly experiment directory An instructor manual and PowerPoint slides of the figures in the book available on a companion website A comprehensive guide to contemporary organic chemistry laboratory principles, procedures, protocols, tools and techniques, Experimental Organic Chemistry, Third Edition is both an essential laboratory textbook for students of chemistry at all levels, and a handy bench reference for experienced chemists.

EXPERIMENTAL ORGANIC CHEMISTRY

Author: SONIA RATNANI,SHRINIWAS GURJAR

Publisher: PHI Learning Pvt. Ltd.

ISBN: 8120346130

Category: Science

Page: 400

View: 7801

Primarily intended for the undergraduate students of science, the book deals with the practical aspects of organic chemistry and discusses how experiments should be done in the laboratory. The book introduces the various types of components used in laboratories and describes basic techniques used for purification. It elaborates different methods of identification of organic compounds, their preparation, and analysis. In addition, it emphasizes qualitative analysis of organic compounds. The book contains essential experiments done in an organic lab and also explains the theoretical background of reactions involved. This book is an attempt to provide students with the often used methods in an easy to understand manner, including explanations of theory, procedures and interpretations of results of the experiments. Besides undergraduate students of science, this book is also useful for the postgraduate students of chemistry. KEY FEATURES : Includes reaction mechanism of each reaction Describes in Appendices safety measures to be taken in laboratory and how to prepare chemical reagents Contains self assessment questions at the end of each chapter.

Experimental Organic Chemistry

Laboratory Manual

Author: Joaquín Isac-García,José A. Dobado,Francisco G. Calvo-Flores,Henar Martínez-García

Publisher: Academic Press

ISBN: 0128039353

Category: Science

Page: 500

View: 6732

Experimental Organic Chemistry: Laboratory Manual is designed as a primer to initiate students in Organic Chemistry laboratory work. Organic Chemistry is an eminently experimental science that is based on a well-established theoretical framework where the basic aspects are well established but at the same time are under constant development. Therefore, it is essential for future professionals to develop a strong background in the laboratory as soon as possible, forming good habits from the outset and developing the necessary skills to address the challenges of the experimental work. This book is divided into three parts. In the first, safety issues in laboratories are addressed, offering tips for keeping laboratory notebooks. In the second, the material, the main basic laboratory procedures, preparation of samples for different spectroscopic techniques, Microscale, Green Chemistry, and qualitative organic analysis are described. The third part consists of a collection of 84 experiments, divided into 5 modules and arranged according to complexity. The last two chapters are devoted to the practices at Microscale Synthesis and Green Chemistry, seeking alternatives to traditional Organic Chemistry. Organizes lab course coverage in a logical and useful way Features a valuable chapter on Green Chemistry Experiments Includes 84 experiments arranged according to increasing complexity

Experimental Organic Chemistry

Author: Clark F. Most

Publisher: Wiley

ISBN: N.A

Category: Science

Page: 608

View: 4553

Acquaints students with all basic laboratory procedures, coordinating enough theory and technique to enable readers to fully comprehend the reactions being studied and the procedures involved. Material is organized in four sections: techniques, experiments, organic qualitative analysis, and appendixes. The first section introduces students to all common organic techniques and provides an illustrative experiment with each. A unique format helps train the research-oriented student to look for relationships that are not immediately apparent. The experiments section moves on to more complex experiments involving synthetic procedures followed by work-up and analysis requiring more than one technique. Instructions are complete and easy to follow, and a set of pre-laboratory experiments encourages students to determine goals before beginning lab work. The appendixes cover less-referred-to techniques: sublimation, density determination, and molecular weight determinations; and contaion a pronunciation guide and a compilation of chemical hazards.

Experimental Organic Chemistry

A Small-scale Approach

Author: Charles F. Wilcox,Mary F. Wilcox

Publisher: Prentice Hall

ISBN: 9780024276919

Category: Science

Page: 542

View: 1526

This text is suitable for second year organic laboratory courses taught in the chemistry department. This thorough introduction to organic laboratory techniques presents an integrated view of the theory underlying technique while aiming to provide an understanding of the techniques rather than mere training in their use. With experiments covering a wide range of scales from micro to standard, this text emphasizes the middle ground, small scale, providing large enough amounts of materials to develop the required manipulative skills while minimizing the costs and hazards of the materials employed.

Experimental Organic Chemistry

A Balanced Approach, Macroscale and Microscale

Author: Jerry R. Mohrig

Publisher: W H Freeman & Company

ISBN: 9780716733300

Category: Science

Page: 733

View: 7913

This laboratory manual seeks to provide a balance between the approaches of microscale and macroscale.

Experimental Organic Chemistry

Standard and Microscale

Author: Laurence M. Harwood,Christopher J. Moody,Jonathan M. Percy

Publisher: Blackwell Publishing

ISBN: 9780632048199

Category: Science

Page: 716

View: 6120

This established text continues to provide a rigorous account of the principles and practice of experimental organic chemistry, taking students from their first day in the laboratory right through to research work. New to this edition, a microscale approach has been integrated into the entire text, alongside conventional manipulations, bringing it in line with current laboratory practice. Maintaining the unique structure of the previous edition, the first half of the book surveys all aspects of safe laboratory practice and the use of a wide range of purification and analytical techniques, particularly spectroscopic analysis. The second half contains easy-to-follow experimental procedures, each designed to illustrate an important reaction type of basic principle of organic chemistry. Tried and tested over the past decade, these experiments are graded according to their complexity and many of these have microscale equivalents. Of prime importance, all aspects of health and safety in the laboratory have been updated according to the latest guidelines and are highlighted throughout the text.